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Agilent Technologies 5975 manuel d'utilisation

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Table des matières du manuel d’utilisation

  • Page 1

    Agilent T echnologies 5975 Series Mass Selective Detectors Site Preparation Guide 5975 Series Site Prep.book Page 1 Thursday, January 31, 2008 9:47 AM[...]

  • Page 2

    Site Prepar ation Guide Notices © Agilent T e chnologies, Inc. 2008 No part of this manual ma y be reproduc ed in any form or by any means (including elec- tronic storage and retrieval or translation into a foreign language) without prior agree- ment and written consent from Agilent T echno logies, Inc. as gov erned by Unite d States and internati[...]

  • Page 3

    Site Preparation Guide 3 Conten ts 1 General Inf ormati on Instrument I dentificati on 6 5975 MSD vers ions 6 Important Safety Warnings 7 Many inte rnal part s of the M SD carry d angerous voltages 7 Electrostatic discharge is a threat to MS D electroni cs 8 Many parts a re dangero usly hot 8 Hydrogen Safety 9 Chemical Safety 10 Safety and Regu lat[...]

  • Page 4

    4 Site Prepar ation Guide V oltage ran ges of ma jor comp onents 23 Power co nfig urat ions 24 Power re quiremen ts 25 Power pl ugs and cor d 2 6 Other electri cal consid eratio ns 27 Air Condi tio ning and Enviro nmenta l Requi rements 28 T emper ature , humidi ty , and alti tude 28 Airbor ne dus t 29 Exhaus t ve nting 29 Fume (exhaust) h ood 30 C[...]

  • Page 5

    5 5975 Series Mass Selective Detectors Site Preparation Guide Agilent T echnologie s 1 Genera l Infor mati on Instrume nt Id entifi cation 6 Import ant Safety W arnings 7 Hydrog en Sa fety 9 Chemical Safety 10 Safety an d Regulator y Certificati ons 11 Cleanin g 1 4 Recyc ling the Pro duct 14 This s e ction pr ovi des inf ormation on h o w t o iden[...]

  • Page 6

    6 Site Prepar ation Guide General In formation Instrument Identification Each 5975 Series Mass Selectiv e Detector ( MSD) is identified by a unique 10-character serial number . This serial number is located on a label on the low er lef t side nea r th e front of the instr u ment. On CI upg rades , a second seri al numbe r is loc ated on the f lo w [...]

  • Page 7

    General Informati on Site Preparation Guide 7 Important Safety W arni ngs Bef ore mo ving on , there are sev eral im port ant saf ety noti ces that y ou should alwa y s k eep in mind when using the 5975 Series M ass S elective D etector . Many interna l parts of the MSD carry danger ous voltages If th e MSD is co nnected to a pow er source, even if[...]

  • Page 8

    8 Site Prepar ation Guide General In formation The use of incorrect or makeshift fuses or the shor t-circuiting of fuse holders creat es a shock ha zard f or t he operator an d can damage t he inst ru ment. Replac e fuse s only wit h fuse s of iden tical cu r rent rati ng and type. Ex cessiv e f luc tuatio ns in the lin e voltage can create a shock[...]

  • Page 9

    General Informati on Site Preparation Guide 9 Hydrogen Safety Hydrogen gas may be used as car rier gas , and/or as fuel for cer t ain G C detec tors. When mixed wit h air , hydrogen can form ex plosive mixt ures. A detaile d discussion of h y drogen safety appears in Chapt er 1 of the Agile nt 5975 MSD Troubleshooting and Maintenance Manual. R ead [...]

  • Page 10

    10 Site Prepar ation Guide General In formation Chemical Safety W A RNING The foreline pump exhaust and split vent exhaust will con tain traces of the chemicals you are analyzing. These could potentially be toxic. V ent the foreline pump exhaust and spl it vent exhaust outside your labora tory or into a fume hood. Be sure to comply with all local e[...]

  • Page 11

    General Informati on Site Preparation Guide 11 Safety and Regulatory Cer tifications The 5975 Series M SD conf o rms to the follo wing saf ety standards: • Canadian Standards Associ a tion (CSA): C AN/CSA–C22.2 No . 61010–1–04 • CSA/N ationally Recognized T est Laboratory (NRTL): UL 61010–1 • International Electrotechnical Commiss ion[...]

  • Page 12

    12 Site Prepar ation Guide General In formation Symbols W arn ings in the man ual or on the instrument mu st be obse rve d during a ll phase s o f ope rat ion, ser vice , an d rep air of th is inst r umen t. F ailu re t o c omply with thes e precau tions violat es s afety st and ards of de sign and t he i nte nded use of the in str umen t. Agi lent[...]

  • Page 13

    General Informati on Site Preparation Guide 13 Electromagnetic compatibility This device complies with t he requiremen ts of CISPR 11. Operat ion is subject to the f ollo wing tw o cond itions: • This de vice ma y not caus e harmful interfer ence. • This de vice must ac cept an y interfe r ence re ceiv e d, in cluding interfer ence that ma y ca[...]

  • Page 14

    14 Site Prepar ation Guide General In formation Cleaning T o clean the unit, dis connect the po wer and wipe do wn wit h a dam p, lint- free cloth. Recycling the Produc t F or recyclin g, cont act y our local Agilen t sales office. 5975 Series Site Prep.book Page 14 Thursday, January 31, 2008 9:47 AM[...]

  • Page 15

    15 5975 Series Mass Selective Detectors Site Preparation Guide Agilent T echnologie s 2 Site Preparation Overview 16 Space and W eight Requireme nts 20 Communi cation s Requireme nts 22 Electr ical Requirements 23 Air Condi tioning and En vironment al Requirements 28 Carrier and Reage nt Gas Requ ire ments 31 Laboratory Supply Require ments 33 Rece[...]

  • Page 16

    16 Site Prepar ation Guide Site Preparation Overview Bef ore the 5975 Series MSD system can be installed, the sit e must be properly prepa red. Site preparat ion include s, but is not li mited to, ensur ing that adequat e facili ties are available. Among th e site requ irement s are: • A dequat e space is available for t he MSD system . • A sui[...]

  • Page 17

    Site Preparation Site Preparation Guide 17 • Com plying with all local la ws (co des, ord inances, and regu lation s) f or mechan ical, build ing, and elec trical distr ibuti on systems, hazar dous was t e disposa l, an d chemi cal s tora ge. Compliance must exist prior to installation. • Pro vidin g lifting equipme nt adequ ate to unload the s[...]

  • Page 18

    18 Site Prepar ation Guide Site Preparation Ag ilent Technolo gies is not re sponsi ble for: • Any task n ot list ed in t he 5975 Series MSD T roubleshooting and Main te nanc e Man ual or the inst a llation guid es f or the G C, dat a syste m, and other accessories • Insta lling helium car rier gas or reagent gas t ank s and regulat ors • Con[...]

  • Page 19

    Site Preparation Site Preparation Guide 19 Other documentat ion Additiona l infor matio n is co nt ained in t he following docum ent at ion: • 5975 Series MSD T roubleshooting and Maintenance Manual • 5975 Series MS D Operation man ual • 6890 Series GC manuals • GC acce ssories (autosam pler , etc. ) manuals • G170 1EA MSD Pr oductivity C[...]

  • Page 20

    20 Site Prepar ation Guide Site Preparation Space and W eight Requi rements Table 2 l ists dim ensi on an d weight infor mat ion for t h e MS D and rel ate d component s. Y our sit e must have enough benc h space for the MSD , GC, dat a system, a nd accessor ies (Figur e 1). In addi tion, there mu st be sufficient space around t he syst em f or ven[...]

  • Page 21

    Site Preparation Site Preparation Guide 21 Ta b l e 2 Product dimens ions Approxima te Dimension s, cm (in) Produc t Heigh t Width Dept h W eight , kg ( lb) 5975 Seri e s MSD • G3170A D iffusion EI MSD 41 (16) 30 (12) 54 (21) 39 (85) • G3171A S tandard turbo EI MSD 41 (1 6) 30 (12 ) 54 (2 1) 39 (8 5) • G3172A P erforma n ce turbo EI MSD 41 (1[...]

  • Page 22

    22 Site Prepar ation Guide Site Preparation Communication s Require ments Te l e p h o n e A tel ephone with a cord long enough t o be used at t he computer wil l allow the MSD ope r ator to commun icate with Agilen t Tech nologi es support personne l. Site LAN network If y ou intend t o conn ect y o ur M SD syste m to your site’s L AN netw ork, [...]

  • Page 23

    Site Preparation Site Preparation Guide 23 Electrical Requirements Y ou are res ponsible f or pro vidin g appr opriate elec trical po we r and po wer outlets f or all of the components in y our 5975 Series MSD system. P o wer cons ider ati ons in clu de: • V olta ge ranges of major components • P o w er configurations • P ow er re quirements [...]

  • Page 24

    24 Site Prepar ation Guide Site Preparation Power configurations Electrical po wer for th e MSD must be single-phas e. The neutral wire cannot be used for safety grounding. The g round wire should car r y zero current ex cept for ground-fau lt cu rren t or st a tic elec tric d ischarge. The en tire sy st em shou ld share a n isola ted, noise-free e[...]

  • Page 25

    Site Preparation Site Preparation Guide 25 Power requirements Table 4 lists the po we r requirements f or t he 5975 Series MSD a n d related equipme nt. Extra po wer cap acity for future additio n s is rec ommended. Each pro duct listed r equir es a d edicated c ircuit. T he gauge contr oller i s po were d b y the MSD. Th e MSD, GC, and data system[...]

  • Page 26

    26 Site Prepar ation Guide Site Preparation Power plugs and cord The MSD is supplied with a po w er cord and plug appropri ate f or the country from which t he order ori ginates. For example, i f an order o riginat es from a Agil ent Technologies s ales off i ce in Ger many , the pow er cord and plug supplie d will be compa tible with the standar d[...]

  • Page 27

    Site Preparation Site Preparation Guide 27 Other electr ical considerat ions Additional electrica l consi deratio ns in clude: • Elec troma gnetic interfe renc e (EMI), such as is genera ted by NM Rs, radi o transmit ters, an d microwa ve link s, may inter fere with system perform ance. • Pr otect the sy stem from stati c elec tricit y by obser[...]

  • Page 28

    28 Site Prepar ation Guide Site Preparation Air Conditioning and Envir onmental Requi rements Air co ndit ionin g cons idera tions inclu de t emperat ure, hu midi ty , air bor ne dust , and exhau st venting. Eac h of thes e is consid ered in more det ai l in the fol low i n g m a t e r i a l . T emperature, humidity , and altitude The 5975 Series M[...]

  • Page 29

    Site Preparation Site Preparation Guide 29 Airborne dust Agilent T echnolog ies recommends a ma ximum ai rborne particle dens ity of 55 μ g/m 3 . If y ou suspect y our site ex ceeds this l imit, co nt act y our local Agilen t T e chnologi es Cust omer Se rvice Organ ization. Cu stom er Engin eers with speci al tr aining and equi pment can tes t fo[...]

  • Page 30

    30 Site Prepar ation Guide Site Preparation See your GC manu als for inform atio n on venting t he spli t vent. Fume (exhaust) hood An auxili ar y work space and fume hood are ne eded for some maint enance procedures. 5975 Series Site Prep.book Page 30 Thursday, January 31, 2008 9:47 AM[...]

  • Page 31

    Site Preparation Site Preparation Guide 31 Carrier and Reag ent Gas Requirements Table 6 list s the spec if ication s for the carr ier and reag ent gases. Pressur es and f l o ws a re as m easur ed at the bulkhe ad f itt ings on t he bac k of t he instr umen t, not at t he g as suppl y. W e recommend that addit ional shut- of f val v es b e install[...]

  • Page 32

    32 Site Prepar ation Guide Site Preparation Regulators, tubing, and fittings Y ou must supply appropriat e regulators for you r car rier and reagen t gas. • Regula tors m ust be dual-s ta ge. • Regul ators must hav e stainless -steel ( not e lastomer ic) diaphr agms. • The y must suppl y gas at the pressure spe cified. • They m ust h ave on[...]

  • Page 33

    Site Preparation Site Preparation Guide 33 Laboratory Suppl y Requirements Laborator y supply requirements vary wit h applicati ons. Cleaning solvents Cleaning t ask s for the M SD require t he followi n g HPLC-g rade (or bette r) solvents: • Methylene chlo ride • Isopropyl alcohol • Meth anol • Ac e t o n e • Wa t e r Proper storag e, ha[...]

  • Page 34

    34 Site Prepar ation Guide Site Preparation Spare parts a nd consumables The supplies and par ts list ed in Table 7 are used in the operati on and maintenance of a 5975 Series MSD sy stem. K eeping these parts on hand can reduc e sys tem do wntime r elate d to ins tr ument ma intenance an d repair . Ta b l e 7 Maintena nce supplies and co nsumabl e[...]

  • Page 35

    Site Preparation Site Preparation Guide 35 Chemical Consu mables PF TBA (EI calib ration fluid) 05971-6 0571 PFDTD (CI calib ration fluid ) 8500-8130 EV AL A (eva luation sa mple) 05990-60045 OFN (Octafluor onapthalene) 5188-5348 OFN 100 fg/µL 5188-5347 Benzop h enone 85 00-5440 PFHT 5188-53 57 Foreline pump oil, P3, 0.5 liter 6040-0621 Gas Filter[...]

  • Page 36

    36 Site Prepar ation Guide Site Preparation 0.5-mm id , 85% V espel 15% graphite, for 0.32-mm id colum ns 5062-3506 0.8-mm id , 85% V espel 15% graphite, for 0.53-mm id colum ns 5062-3538 GC in let 0.27-mm id, 90% V espel 10 % graph ite, for 0. 10-mm id colum ns 5062-3518 0.37-mm id, 90% V espel 10 % graph ite, for 0. 20-mm id colum ns 5062-3516 0.[...]

  • Page 37

    Site Preparation Site Preparation Guide 37 Receiving t he System When you r MSD sys tem is d elivere d, it is your resp onsi bilit y t o provide for remo val of the ship ping containers fr om the truck and thei r storage until inst al lation. Cont act your Ag ilent Techno logies s ervice repres ent ative a s soon as your shi pment ar rives t o ar r[...]

  • Page 38

    38 Site Prepar ation Guide Site Preparation Storage It is your respo nsibi lity to store the c ont ainer s unti l inst al lation . If your site does no t hav e adequat e st orage spac e, the c ont ainers may be stored at your expense i n a b onded wa rehouse. Allow space for data syst em a nd ac cessor y cont ainer s t oo. The environment i n the s[...]

  • Page 39

    Site Preparation Site Preparation Guide 39 Installation and V erification Installation Once the in stallatio n has beg un, it sho uld pro gress in a time ly manner to completion. D elays due t o inad equat e site preparation could c ause loss of instr ument use d uring t he warrant y period. In e xtreme c ases, Agil ent T e chnologies may ask to be[...]

  • Page 40

    40 Site Prepar ation Guide Site Preparation Sensitivity specifications See the appro priate sensit ivity specifications f or your inst rument type. See the Agile nt T echnolo gies W eb site at http://www .agilent .com/ch em. NOTE SIM performance verification is not perf ormed at inst allation and must be purchased if desir ed. 5975 Series Site Prep[...]

  • Page 41

    41 5975 Series Mass Selective Detectors Site Preparation Guide Agilent T echnologie s A Power Cords This appendix sho ws t he pow er cords availabl e for the 5975 Series MSD. See page 26 for inf or mation a bout ensuring that the correct po wer cord is s upplied wit h your syst em . US and Canada, NEMA 6- 15P (Part number 8120 -6825) Europea n Powe[...]

  • Page 42

    42 Site Prepar ation Guide Power Cords Denm ark/Gr eenla nd, IEC 309 (Pa rt num ber 8120 -399 7) Austr alia/New Ze aland, AS 31 12-198 1 (Part numbe r 8120-136 9) India/S outh Africa , BS 546 (Par t numb er 8120 -4211) Israe l, SI 32 (Par t number 8120-5 182) Japan, NEMA L6-20 P (Part number G2025-601 89) 5975 Series Site Prep.book Page 42 Thursday[...]

  • Page 43

    5975 Series Site Prep.book Page 43 Thursday, January 31, 2008 9:47 AM[...]

  • Page 44

    Agilent T echnologie s © Agilent T echnologies, Inc . Printed in USA, J a nuary 2008 5975 Series Site Prep.book Page 44 Thursday, January 31, 2008 9:47 AM[...]