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Teledyne T201 manuel d'utilisation

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Table des matières du manuel d’utilisation

  • Page 1

    MANUAL ADDENDUM MODEL T201 AMMONIA ANAL YZER (For use with the T200 Op erators Manual, P/N 06858) TELEDYNE ADVANCED POLLUTION INSTRUMENTATION (TELEDYNE-API) 9480 CARROLL PARK DRIVE SAN DIEGO, CA 92121-5201 TOLL-FREE: 800-324-5190 FAX: 858-657-9816 TEL: 858-657-9800 E-MAIL: api-sales@teledyne.com WEB SITE: www.teledyne-api.com Copyright 2011-2013 07[...]

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  • Page 3

    07271B DC N6646 i ABOUT THIS MANUAL This addendum is to be used in conjunction with the T200 NOx Analyzer manual, p/n 06858; for operating the T201 analyz er; it includes document(s) as listed below. Part No. Name/Description 07356 T201 Spare Parts List (in Section 7.0) Note: Please refer to our Website or Sales for more recent updates. Note We rec[...]

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    ii 07271B DC N6646 This page intentionally left blank.[...]

  • Page 5

    Teledyne API Model T201 NH 3 Analyzer Operat or Ma nual T201 Ammonia Analyzer 07271B DC N6646 iii SAFETY MESSAGES Important safety messages are provided throughout this manual for the purpose of avoiding personal injury or instrument damage. Please read these mes sages carefully. Each safety message is associat ed with a safety alert symbol, and ar[...]

  • Page 6

    iv 07271B DC N6646 CONSIGNES DE SÉCURITÉ Des consignes de sécurité important es sont fournies tout au long du présent manuel dans le but d’év iter des blessures corporelles ou d’endommager les instruments. Veuillez lire attentivem ent ces consignes. Chaque consigne de sécurité est re présentée par un pictogramme d’alerte de sécurit[...]

  • Page 7

    07271B DC N6646 v TABLE OF CONTENTS MODEL T201 AMMO NIA ANALYZER ............................................................. I CONSIGNES DE SÉCURI TÉ ......................................................................... IV 1.0 T201 AMMONI A ANALYZER ................................................................. 7 1.1 Theory of Operation [...]

  • Page 8

    vi 07271B DC N6646 Table 2-4. NO Calibration Procedur e - NO Gas thr ough the SPAN Port ....................... 19 Table 2-5. Confirming Amm onia Converter Effici ency ................................................... 21 Table 2-6. NH 3 Calibration Procedure – NH 3 Gas through t he SAMPLE Port ............... 22 Table 2-7. NH 3 Calibration Proc[...]

  • Page 9

    07271B DC N6646 7 1.0 T201 AMMONIA ANALYZER This manual is to be used in conjunction with the T200 NO x Analyzer manual, p/n 06858 supplied with this instrument. It is i mportant that you familiarize yourself with the workings of the NO x analyzer be fore proceeding with NH 3 measurements. The T201 ammonia analyzer consists of a modified T200 nitro[...]

  • Page 10

    T201 Ammonia Analyzer Teledyne API Model T201 NH 3 Analyzer Operator Ma nual 8 07 271B DCN6646 Figure 1-1. T201 Pneumatic Connection Diagra m w/External Calibrator Option (ECO)[...]

  • Page 11

    Teledyne API Model T201 NH 3 Analyzer Operat or Ma nual T201 Ammonia Analyzer 07271B DC N6646 9 Figure 1-2. T201 and M501 NH 3 Pneumatic Flow M501NH3 TNX OUT TN OUT SPAN GAS INLET Zero Gas Valve Span Gas Valve Sample Gas Valve ZERO AIR INLET SAMPLE GAS INLET PUMP Optional Sample Filter P/N 016300800, 1 Micron PTFE Or P/N 055710000, 0.5 Micron SS TN[...]

  • Page 12

    T201 Ammonia Analyzer Teledyne API Model T201 NH 3 Analyzer Operator Ma nual 10 07271B DC N6646 1.1 T HEORY OF O PERATION The Teledyne-API Model T201 analyzer measures ammonia by oxidizing it to nitric oxide by the f ollowing reaction: 4NH 3 + 5O 2  4NO + 6H 2 O The resulting nitric ox ide is then measured by the chemiluminescent reaction with o[...]

  • Page 13

    Teledyne API Model T201 NH 3 Analyzer Operat or Ma nual T201 Ammonia Analyzer 07271B DC N6646 11 The ammonia converter efficiency factor (NH 3 _CE_FACTOR1) is discussed in more deta il in Section 2.3 of this manual. The conversion efficiency of the M501 NH 3 should be checked prior to starting long term tests. Both efficiency factors ca n be access[...]

  • Page 14

    T201 Ammonia Analyzer Teledyne API Model T201 NH 3 Analyzer Operator Ma nual 12 07271B DC N6646 As can be seen from the above reactions, the calculation of the ammonia concentration and overall calibration of the instrument must be done carefully, if accurate ammonia conc entrations are to be measured. 1.2 S PECIAL C ONSIDERATIONS F OR A MMONIA M E[...]

  • Page 15

    Teledyne API Model T201 NH 3 Analyzer Operat or Ma nual T201 Ammonia Analyzer 07271B DC N6646 13 1.4 T201 A NALYZER S PECIFICATIONS Table 1-1. T201 Operating Specifications Ranges Min: 0-50 ppb Full scale Max: 0-2000 ppb Full scale (selecta ble, independent NH 3 , NO, NO 2 , NOx ranges supported) Measurement Units PPB, PPM, microgram/m 3 , milligra[...]

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    07271B DC N6646 15 2.0 CALIBRATION PROCEDURE This section begins with a high-level overview of the calibration procedur e for the T201 analyzer. Details are provided starting in Section 2.1.  First, take the time to read the T200 manual to familiarize yourself with the Chemiluminescenc e process. It is importan t to remember that t he analyzer i[...]

  • Page 18

    Calibration Procedure Teledyne API Model T201 NH 3 Analyzer Operator Ma nual 16 07271B DC N6646 2.1 Z EROING THE A NALYZER The analyzer can be zeroed by either applying zero air straight to th e sample port or through the optional Ze ro/Span valves, if installed. It is important to remem ber that if the analyzer was previously sam pling ammonia gas[...]

  • Page 19

    Teledyne API Model T201 NH 3 Analyzer Operat or Ma nual Calibration Procedure 07271B DC N6646 17 Table 2-2. Zero Calibration Procedu re - Z ero Gas through ZERO Port Step No. Action Comment 1. Press CALZ The T201 enters the calib rate mode from sample mode. The zero gas is s upplied through the ZERO inlet port on the rear panel of the M501 NH 3 . 2[...]

  • Page 20

    Calibration Procedure Teledyne API Model T201 NH 3 Analyzer Operator Ma nual 18 07271B DC N6646 Table 2-3. NO Calibration Procedure – NO Gas through the SAMPLE Port Important: Each channel (TN x and NO x ) must be Spanned individually Step No. Action Comment 1. Press CAL The T201 enters the calib rate mode from sample mode. Confirm that excess NO[...]

  • Page 21

    Teledyne API Model T201 NH 3 Analyzer Operat or Ma nual Calibration Procedure 07271B DC N6646 19 Table 2-4. NO Calibration Procedure - NO Gas through the SPAN Port Step No. Action Comment 1. Press CALS The T201 enters the calib rate mode from sample mode. The NO gas is suppl ied through the SPAN inlet port on the rear panel of the M501 NH 3 . 2 Tab[...]

  • Page 22

    Calibration Procedure Teledyne API Model T201 NH 3 Analyzer Operator Ma nual 20 07271B DC N6646 The most important criterion an indi vidual can avail them selves of when spanning an analyzer with ammonia gas is “patien ce”. Ammonia is a very sticky gas and the response of the analyzer/calibration system depends on a number of factors. The follo[...]

  • Page 23

    Teledyne API Model T201 NH 3 Analyzer Operat or Ma nual Calibration Procedure 07271B DC N6646 21 Table 2-5. Confirming A mmonia Converter Efficiency Step No. Action Comment 1. Press CAL The T201 enters the calib rate mode from Sample mode. 2. Channel Selection Press TN X then Press ENTR . 3. Range Selection Press LOW range then Press ENTR. 4. Press[...]

  • Page 24

    Calibration Procedure Teledyne API Model T201 NH 3 Analyzer Operator Ma nual 22 07271B DC N6646 Table 2-6. NH 3 Calibration Procedure – NH 3 Gas through the SAMPLE Port Note In the example outlined abov e, the displayed ammonia concentration is being increased by 2.27%. Newer M501 NH 3 conv erters should have efficiency values very close to 1.00.[...]

  • Page 25

    Teledyne API Model T201 NH 3 Analyzer Operat or Ma nual Calibration Procedure 07271B DC N6646 23 Table 2-7. NH 3 Calibration Procedure – NH 3 Gas through the SPAN Port Step No. Action Comment 1. Press CALS The T201 enters the calib rate mode from Sample mode. The ammonia gas is supplied through the SPAN inlet port on the rear panel of the M501 NH[...]

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    Calibration Procedure Teledyne API Model T201 NH 3 Analyzer Operator Ma nual 24 07271B DC N6646 This page intentionally left blank.[...]

  • Page 27

    07271B DC N6646 25 3.0 CONFIGURABLE ANALOG OUTPUT OVERVIEW There are three different methods to extract concentration data from the analyzer: internal data acquisition syst em (DAS), hyperlink, or strip chart . DAS The user can set up an internal DAS configuration either through the user display or using TAPI’s windows based softwa re called APIC[...]

  • Page 28

    Configurable Analog Outpu t Overview Teledyne API Model T201 NH 3 Analyzer Operator Ma nual 26 07271B DC N6646 Table 3-2. Analog Output Pin-Outs PIN ANALOG OUTPUT VOLTAGE SIGNA L CURRENT SIGNAL 1 V Out I Out + 2 A1 Ground I Out - 3 V Out I Out + 4 A2 Ground I Out - 5 V Out I Out + 6 A3 Ground I Out - 7 V Out N/A 8 A4 Ground N/A Additionally A1, A2 [...]

  • Page 29

    07271B DC N6646 27 4.0 MAINTENANCE SCHEDULE The maintenance requirements of th e T201 are the same as a standard T200 NO x analyzer but with additional maintenance items ( Table 4-1). Please refer to Section 13 in the T200 Operator Manual for the T200 maintenance schedule and for main tenance and repair procedures. The T201 requires the following a[...]

  • Page 30

    Maintenance Schedule Teledyne API Model T201 NH 3 Analyzer Operator Ma nual 28 07271B DC N6646 Table 4-2. M501 NH 3 Converter Rebuild Parts List Part No. Description KIT000193 RETROFIT, M501 NH 3 INNER TUBE w/SCREEN KIT000139 REBUILD, CERAMIC BUSHINGS, M501 NH 3 HE0000007 CERAMIC HEATER, 220W@60V M501XX 4.2 R EPLACING THE C ATALYTIC C ARTRIDGE 1. T[...]

  • Page 31

    Teledyne API Model T201 NH 3 Analyzer Operat or Ma nual Maintenance Schedule 07271B DC N6646 29 4.3 R EPLACING THE T HERMOCOUPLE The following instructions provide th e necessary information to replace the existing thermocouple. Figure 4-2 is provided for reference. You m ust obtain the following re placement parts kit from TAPI:  010820000 , Ty[...]

  • Page 32

    Maintenance Schedule Teledyne API Model T201 NH 3 Analyzer Operator Ma nual 30 07271B DC N6646 Once you have the right too ls and parts, replace the thermocouple as follows: 1. Ensure power is removed from the M501 NH 3 Converter. If the Converter has been operational you will need to wait for at least 2 hours for the Converter oven to cool before [...]

  • Page 33

    Teledyne API Model T201 NH 3 Analyzer Operat or Ma nual Maintenance Schedule 07271B DC N6646 31 18. After the Auto-Tune process is completed, verify that the “process” temperature is indicating that the desired temperature is stable and being regulated. The converter is now ready for operation. 4.4 A UTO Z ERO F LOW C HECK Since the T201 is an [...]

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    Maintenance Schedule Teledyne API Model T201 NH 3 Analyzer Operator Ma nual 32 07271B DC N6646 This page intentionally left blank.[...]

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    07271B DC N6646 33 5.0 ALARMS AND CAUTIONS Please refer to the T200 Operation Ma nual for a functiona l block diagram of the analyzer. 5.1 A LARM During initial warm up the internal Zero/Span factory op tion may exhibit a “Block Temperature” warning. This can be cleared once the block temperature stabilizes at 50 degrees Ce lsius. The block tem[...]

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    Alarms and Cautions Teledyne API Model T201 NH 3 Analyzer Operator Ma nual 34 07271B DC N6646 This page intentionally left blank.[...]

  • Page 37

    07271B DC N6646 35 6.0 CALCULATING MOLY CONVERTER EFFICIENCIES 6.1 P URPOSE To provide instructions on how to cal culate the efficiency of a Moly converter when using a GPT method of testing converters, by using the US EPA method, where the actual concentr ation of ozone is not a factor in the accuracy of the calculation of the converter efficiency[...]

  • Page 38

    Calculating Moly Converter Efficiencies Teledyne API Model T201 NH 3 Analyzer Operat or Ma nual 36 07271B DC N6646 3. The first gas check is t o test to see how much the converter is eating NO gas or out gassing NO gas. Bypass the converter in th e machine, by placing a short piece of tubing in place of the converter. Perform a straight dilution wi[...]

  • Page 39

    07271B DC N6646 37 MOLY TEST DATA SHEET Line # TEST RESULT 2 LEAK-CHECK (WHEN HOT) YES / NO 3 NO X RESPONSE (MOLY BYPASSED) __________ 4 NO X RESPONSE (MOLY IN-LINE) __________ 5 OUT-GASSING / EATING (NO – NO X ) _________ _ (>-5 PPB, <5 PPB) 6 (NOx ORIG ) (NO X mode, O 3 off) __________ PPB 7 (NOx REM ) (NO X mode, O 3 on) __________ PPB 8[...]

  • Page 40

    Calculating Moly Converter Efficiencies Teledyne API Model T201 NH 3 Analyzer Operat or Ma nual 38 07271B DC N6646 This page intentionally left blank.[...]

  • Page 41

    07271B DC N6646 39 7.0 T201 SPARE PARTS LIST This section lists the spare parts for the T201; however, due to the dynamic nature of spare parts numbe rs, it is recommended that you refer to our Website or contact Sales for recent updates. (Reference: 07356 29 March 2012, 12:17PM) PARTNUMBER DESCRIPTION 000940100 CD, ORIFICE, .003 GREEN 000940400 CD[...]

  • Page 42

    T201 Spare Parts List Teledyne API Model T201 NH 3 Analyzer Operat or Manual 40 07271B DC N6646 (Reference: 07356 29 March 2012, 12:17PM) PARTNUMBER DESCRIPTION 049310100 PCA,TEC DRIVER,PMT,(KB) 051211000 ASSY, O3 DESTRUCT W/FTGS (MNFLD - EXH) * 052930200 ASSY, BAND HEATER TYPE K, NOX 055710000 ASSY, FLT, INLINE SS, 3/8” CONN, 0.5 MIC 058021100 P[...]

  • Page 43

    Teledyne API Model T201 NH3 Analyzer Operator Manual 07271B DC N6646 41 (Reference: 07356 29 March 2012, 12:17PM) PARTNUMBER DESCRIPTION HW0000685 LATCH, MAGNETIC, FRONT PANEL KIT000095 AKIT, REPLACEMENT COOLER KIT000219 AKIT, 4-20MA CURRENT OUTPUT KIT000253 ASSY & TEST, SPARE PS37 KIT000254 ASSY & TEST, SPARE PS38 OR0000001 ORING, 2-006VT [...]

  • Page 44

    T201 Spare Parts List Teledyne API Model T201 NH 3 Analyzer Operat or Manual 42 07271B DC N6646 This page intentionally left blank.[...]