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Teledyne 201A manual

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Table of contents for the manual

  • Page 1

    MANUAL ADDENDUM MODEL 201A AMMONIA ANALYZER TELEDYNE ADVANCED POLLUTION INSTRUMENTATION (T-API) 9480 CARROLL PARK DRIVE SAN DIEGO, CA 92121-5201 TOLL-FREE: 800-324-5190 FAX: 858-657-9816 TEL: 858-657-9800 E-MAIL: api-sales@teledyne.com WEB SITE: www.te le dy ne -ap i.c om 04689 REV. B1 Copyright 2005 T-API Inc. 12 September, 2005[...]

  • Page 2

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 SAFETY MESSAGES Your safety and the safety of others is very im portant. We have provided many important safety messages in this manual. Please read these messages carefully. A safety message alerts you to potential hazards that could hurt you or others. Each safety message i[...]

  • Page 3

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 TABLE OF CONTENTS SAFETY MESSAGES ....................................................................................................... 1 TABLE OF CONTENTS ................................................................................................... 2 1 .0 M201A AMMON[...]

  • Page 4

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 LIST OF FIGURES F IGURE 1 - M201A A MMONIA A NALYZER – B LOCK D IAGRAM ................................................................. 21 F IGURE 2 - M201A E XTERNAL P NEUMATIC C ONNECTION D IAGRAM WITH ECO (E XTERNAL C ALIBRATOR O PTION ) ................................[...]

  • Page 5

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 LIST OF TABLES T ABLE 2.1 - Z ERO C ALIBRATION P ROCEDURE - Z ERO G AS T HROUGH THE S AMPLE P ORT ......................... 11 T ABLE 2.2 - E NTER THE E XPECTED S PAN G AS C ONCENTRATIONS P ROCEDURE ......................................... 11 T ABLE 2.3 - S PAN C ALIBRATION [...]

  • Page 6

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 5[...]

  • Page 7

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 1.0 M201A AMMONIA ANALYZER This manual is to be used in conjunction with the M200A NOx Analyzer manual p/n 02246 supplied with this instrument. The M201A Ammonia Analyzer consists of a modified M200A Nitrogen Oxides Analyzer and M501NH Ammonia Converter: A functional block di[...]

  • Page 8

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 converts some of the ammonia to NO, t hus the TN channel data contains a small ammonia signal. Secondly, the ammonia conv erter does not convert all of the ammonia or ambient NO2 to NO. Finally, the high te mperature in the ammonia converter causes the oxygen and nitrogen in [...]

  • Page 9

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 Do NOT use copper tubing or fittings designed for household plumbing. Use ONLY Chromatography grade (cleaned, passivated) stainless steel tubing Use ONLY Glass tubing for sample inlet manifold. These rules apply also to your calibrator’s inte rnal plumbing. Verify that the [...]

  • Page 10

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 1.2 M201A Analyzer Specifications Ranges 0-50 to 0-2000 ppb in 1 ppb increments Range Modes Single, Independent, AutoRange Noise at Zero 1 0.5 ppb RMS Noise at Span 1 < 1.0% of reading above 50 ppb Lower Detectable Limit 1 ppb RMS Zero Drift 3 2 ppb / 24 hours Span Drift &[...]

  • Page 11

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 2.0 CALIBRATION PROCEDURE Calibration of the M201A is done by first calibrating the TN and TNx channels with NO span gas diluted with zero air. In the second phase of calibration, ammonia span gas is introduced to measure the overall system e fficiency for NH3 conversion. Unl[...]

  • Page 12

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 Table 2.1 - Zero Calibration Procedure - Zero Gas Through the Sample Port Step No. Action Comment 1. Press CAL The M201A enters the calibrate mode from sample mode. Input zero gas through the sample port. 2. Wait 20 min Wait for reading to stabilize at zero value. 3. Press ZE[...]

  • Page 13

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 Table 2.3 - Span Calibration Procedure - Span Gas thru Sample Port Step No. Action Comment 1. Press CAL The M201A enters the calibrate mode. Input NO span gas through the sample port. 2. Press CAL-CONV-SET Set the converter efficiency parameter to 1.0000, then press ENTR-EXIT[...]

  • Page 14

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 2.1.1 Zero/Span Calibration with Z/S Valves or ECO Option The zero gas enters through the zero gas inle t port on the rear panel. Make sure that the umbilical cord that makes the cont rol connections between the analyzer and the converter is connected (see Figure 2 below). Th[...]

  • Page 15

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 Table 2.5 - Enter the Expected Span Gas Concentrations Procedure Step No. Action Comment 1. Press CAL- CONC- TNX This key sequence causes the M201A to prompt for the expected TNX concentration. Enter the TNX span concentration value by pressing the key under each digit until [...]

  • Page 16

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 Table 2.6 - CALS - Span Cal Procedure - Gas from rear panel span gas inlet Step No. Action Comment 1. Press CALS The M201A enters the calibrate mode. The Z/S valves are activated to route span gas into the analyzer. 2. Press CAL-CONV-SET Set the converter efficiency parameter[...]

  • Page 17

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 2.1.3 NH3 Calibration Since the system efficiency is less than 100%, it is necessary to determine a conversion efficiency factor for ammonia and enter it into the system. 1. Set the converter efficiency to 1.0000 by: Press CAL-CONC-CONV- SET on the keyboard Press the keys und[...]

  • Page 18

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 The instrument is now fully calibrated. 2.1.4 Channel Calibration Quality After the ammonia channel is calibrated via the converter efficiency parameter, it is important to check the calibration by sampling the NH3 calibration gas and confirming that the instrument responds w[...]

  • Page 19

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 3.0 MAINTENANCE SCHEDULE 3.1 M201A Maintenance Schedule The maintenance requirements of the M201A are essentially like a standard M200A NOx analyzer. Please refer to Table 8-1 in the M200A Operator Manual for the M200A maintenance schedule. In Table 3.1 below, there are the e[...]

  • Page 20

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 Table 3.2 – M501NH Converter Rebuild Parts List Part No. Description KIT000191 Converter Rebuild Kit KIT000139 Ceramic Bushings HE0000007 Ceramic Heater 220W 60 VAC Procedure: 1. Turn off power to the converter and allow to cool . IT IS VERY IMPORTANT THAT THE CONVERTER BE [...]

  • Page 21

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 3.3 AutoZero Flow Check Since the M201A is an ammonia analyzer, the flow through the AutoZero orifice is especially important. Check the AutoZero flow as follows: 1. This procedure should be performed with the sample pump running. 2. Fold down the rear panel on the M201A cha [...]

  • Page 22

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 Figure 1 - M201A Ammonia Analyzer – Block Diagram 21[...]

  • Page 23

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 MODULE AIR ZERO FROM SPAN 02522 UMBILICAL CORD TO VACCUM PUMP POWER UMBILICAL TO CONV CONV FROM UMBILICAL SS TUBING GAS INLET PRESSURE OUT EXHAU ST SAMPLE IN TNX OUT TN TN OUT OUT ZERO AIR SS TUBING CAL GAS OUT NO SPAN GAS NH3 SPAN GAS 50 PSIG MAX CYL 1 IN CYL 2 IN ZERO AIR I[...]

  • Page 24

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 Figure 3 - M201A Pneumatic Diagram Basic 23[...]

  • Page 25

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 Figure 4 - M201A Pneumatic Diagram Z/S Option 24[...]

  • Page 26

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 Figure 5 - M201A Pneumatic Diagram External Calibrator Option (ECO) 25[...]

  • Page 27

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 Figure 6 – M501NH Converter Cartridge 26[...]

  • Page 28

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 27[...]

  • Page 29

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 4.0 M201A SPARE PARTS LIST 000940400 Orifice, 4 mil, 80 cc, Rx Cell 000940600 Orifice, 10 mil, 500 cc, Rx Cell 002270100 Gasket (Rx Cell) Qty. 12 002730000 Window 665 NM 002761020 CPU Board (201A AMX)) 003290000 Thermistor Assembly 004020200 Flow/Pressure Sensor Board 0051403[...]

  • Page 30

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 M201A Spare Parts List (cont.) 016810200 O3 Generator Assembly for M200A/200AH Low Output 017230000 Dryer Material, Drierite 018720000 Welded Moly Conv. Assy, w/ O3 Scrubber, w/ valves 021070000 PMT Pre-amplifier Board Assembly 022300000 DC Power Supply Board 024710000 Tubing[...]

  • Page 31

    Teledyne API Model 201A NH 3 Analy zer Instruction Manual, 04689, Rev. B1 M201A Spare Parts List (cont.) KIT000129 Welded Moly, Cartridge only KIT000191 Rebuild, NH3 INNER TUBE & CATALYST OR0000001 O-Ring, Flow Control OR0000002 O-Ring, Bearing, Cell OR0000010 O-Ring, S, O3 Generator OR0000012 O-Ring, Permeation Oven-Units with IZS OR0000014 O-[...]