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Teledyne M201E manual

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Table of contents for the manual

  • Page 1

    MANUAL ADDENDUM MODEL M201E AMMONIA ANAL YZER (For use with the M200E Operators Manual, P/N 04410) TELEDYNE ADVANCED POLLUTION INSTRUMENTATION (TELEDYNE-API) 9480 CARROLL PARK DRIVE SAN DIEGO, CA 92121-5201 TOLL-FREE: 800-324-5190 FAX: 858-657-9816 TEL: 858-657-9800 E-MAIL: api-sales@teledyne.com WEB SITE: www.teledyne-api.com Copyright 2006-2012 0[...]

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  • Page 3

    05206H DCN5910 i ABOUT THIS MANUAL This manual is an addendum that supplem ents the M200E NOx Analyzer manual, p/n 04410; it includes document(s) as listed below. Part No. Name/Description 06185H M201E Spare Parts List (in Section 6.0) Note: Please refer to our W ebsite or Sales for more recent updates. NOTE We recommend that this ma nual and the M[...]

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    ii 05206H DCN5910 This page intentionally left blank.[...]

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    Teledyne API Model M201E NH 3 Analyzer Operator Manual M201E Amm onia Analyzer 05206H DCN5910 iii SAFETY MESSAGES Your safety and the safety of others is very important. We have provided many safety messages throughout this manual; please read these messages carefully. A safety message alerts you to potential hazards that could hurt you or others. [...]

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    iv 05206H DCN5910 This page intentionally left blank.[...]

  • Page 7

    05206H DCN5910 v TABLE OF CONTENTS 1.0 M201E AMMONI A ANALYZER ............................................................. 7 1.1 Theory of Operation ...................................................................................................... 10 1.1.1 Minim izing PMT Drift .................................................................[...]

  • Page 8

    vi 05206H DCN5910 Figure 3-6. Analog Output Manual Calibration ............................................................................ 33 Figure 3-7. Analog Output Reco rder Offset Calibration .............................................................. 34 Figure 4-1. Catalytic Cartridge ......................................................[...]

  • Page 9

    05206H DCN5910 7 1.0 M201E AMMONIA ANALYZER This manual is to be used in conjunction w ith the M200E NO x Anal yzer manual, p/n 04410 supplied w ith this in strument. It is important that you familiarize yourself with the workings of the NO x analyzer before proceeding with NH 3 measurement s. The M201E ammonia analyzer consists of a modified M200E[...]

  • Page 10

    M201E Ammonia Analyzer Teledyne API Model M201E NH 3 Analyzer Operator Manual 8 05206H DCN5910 Figure 1-1. M201E Pneumatic Connection Diagra m with External Calibrator Option (ECO)[...]

  • Page 11

    Teledyne API Model M201E NH 3 Analyzer Operator Manual M201E Amm onia Analyzer 05206H DCN5910 9 Figure 1-2. M201E and M501 NH 3 , Pneumatic Flow[...]

  • Page 12

    M201E Ammonia Analyzer Teledyne API Model M201E NH 3 Analyzer Operator Manual 10 05206H DCN5910 Figure 1-3. M201E and M501 NH 3 , with Zero and Span Valv e Options Pneumatic Flow 1.1 T HEORY OF O PERATION The Teledyne-API Model M201E analyzer measures ammonia by oxidizing it to nitric oxide by the following reaction: 4NH 3 + 5O 2  4NO + 6H 2 O T[...]

  • Page 13

    Teledyne API Model M201E NH 3 Analyzer Operator Manual M201E Amm onia Analyzer 05206H DCN5910 11 and registered as NO x . This location provides the drier with continuous flow, thereby allowing it to stabilize faster. Note: Due to the Nafion® drier, the anal yzer has a maximum ammonia range of 2.0 PPM. The calculated gas concentrations, a mmonia a[...]

  • Page 14

    M201E Ammonia Analyzer Teledyne API Model M201E NH 3 Analyzer Operator Manual 12 05206H DCN5910 signal. This process improves zero base line stability by minimizing the effect of PMT sensor drift. 1.1.2 Purging the Reaction Cell As with many chemic al reactions the conv er sion of ammonia in the presence of other oxides of nitrogen is complicated. [...]

  • Page 15

    Teledyne API Model M201E NH 3 Analyzer Operator Manual M201E Amm onia Analyzer 05206H DCN5910 13 These rules apply also to your calibrat or’s internal plumbing. It is highly recommended that you use a M 702SS calib rator in c onjunction with the M201E. The calibrator has s tainles s steel plumbing through out. The M700 calibrator contains Teflon [...]

  • Page 16

    M201E Ammonia Analyzer Teledyne API Model M201E NH 3 Analyzer Operator Manual 14 05206H DCN5910 1.4 M201E A NALYZER S PECIFICATIONS Table 1-1. M201E Operating Specifications Ranges 0-50 to 0-2000 ppb in 1 ppb increments (selectable, independent NH 3 , NO, NO 2 , NOx ranges supported) Measurement Units PPB, PPM, microgram/m 3 , milligram/m 3 (user s[...]

  • Page 17

    05206H DCN5910 15 2.0 CALIBRATION PROCEDURE This section begins with a high-level ov ervi ew of the c alibration procedure for t he M201E analyzer. Details are pr ovided starting in Section 2.1:  First, take the time to read the M200E manual to familiarize yourself with the Chemiluminescence process. It is important to remember that t he analyze[...]

  • Page 18

    Calibration Procedure Teledyne API Model M201E NH 3 Analyzer Operator Manual 16 05206H DCN5910 The first time bottled ammonia is connected to the gas dilution system, regulator/calibrator, the TNx readi ng may take a number of hours to stabilize. 2.1 Z EROING T HE A NALYZER The analyzer can be zeroed by either applying zero air straight to the samp[...]

  • Page 19

    Teledyne API Model M201E NH 3 Analyzer Operator Manual Calib ration Procedure 05206H DCN5910 17 Table 2-2. Zero Calibration Procedu re - Z ero Gas Through ZERO Port Step No. Action Comment 1. Press CALZ The M201E enters the cali brate mode from sample mode. The zero gas is s upplied through the ZERO inlet port on the rear panel of the M501 NH 3 ,. [...]

  • Page 20

    Calibration Procedure Teledyne API Model M201E NH 3 Analyzer Operator Manual 18 05206H DCN5910 operator then manua lly spans the TN x and NO x channels individually through the user interface. The following Tables out line the manual steps necessary to span the analyzer. Table 2-3. NO Calibration Procedure – NO Gas Through the SAMPLE Port Importa[...]

  • Page 21

    Teledyne API Model M201E NH 3 Analyzer Operator Manual Calib ration Procedure 05206H DCN5910 19 Table 2-4. NO Calibration Procedure - NO Gas through the SPAN Port Step No. Action Comment 1. Press CALS The M201E enters the cali brate mode from sample mode. The NO gas is suppl ied through the SPAN inlet port on the rear panel of the M501 NH 3 ,. 2 Ta[...]

  • Page 22

    Calibration Procedure Teledyne API Model M201E NH 3 Analyzer Operator Manual 20 05206H DCN5910 2.3 S PANNING T HE A NALYZER W ITH A MMONIA G AS The most important criteri on an individual can avail th emselves of when spanning an analyzer with ammonia gas is “patience”. A mmonia is a very sticky gas and the response of the analyze r/calibration[...]

  • Page 23

    Teledyne API Model M201E NH 3 Analyzer Operator Manual Calib ration Procedure 05206H DCN5910 21 Table 2-5. Confirming Ammonia Converter Efficiency Step No. Action Comment 1. Press CAL The M201E enters the calibrate mode from Sample mode. 2. Channel Selection Press TN X then Press ENTR . 3. Range Selection Press LOW range then Press ENTR. 4. Press C[...]

  • Page 24

    Calibration Procedure Teledyne API Model M201E NH 3 Analyzer Operator Manual 22 05206H DCN5910 Table 2-6. NH3 Calibration Procedure – NH3 Gas Through The SAMPLE Port  Note: In the example outlined above, the displayed ammonia concentration is being increas ed by 2.27%. Newer M501 NH 3 , converters should have efficiency values very close to 1.[...]

  • Page 25

    Teledyne API Model M201E NH 3 Analyzer Operator Manual Calib ration Procedure 05206H DCN5910 23 Table 2-7. NH3 Calibration Procedure – NH3 Gas through the SPAN Port Step No. Action Comment 1. Press CALS The M201E enters the cali brate mode from Sample mode. The ammonia gas is supplied through the SPAN inlet port on the rear panel of the M501 NH 3[...]

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    Calibration Procedure Teledyne API Model M201E NH 3 Analyzer Operator Manual 24 05206H DCN5910 This page intentionally left blank.[...]

  • Page 27

    05206H DCN5910 25 3.0 CONFIGURABLE ANALOG OUTPUT OVERVIEW There are three different me thods to extract concentrat ion data from the E- Series analyzers. By one method, the oper ator can set up an iDas (inter nal data acquisition) configuration eith er through the user displa y or using TAPI’s windows based software called APICO M. The analyzer s[...]

  • Page 28

    Configurable Analog Outpu t Overview Teledyne API Model M201E NH 3 Analyzer Operator Manual 26 05206H DCN5910 Table 3-2. Analog Output Pin-Outs PIN ANALOG OUTPUT VOLTAGE SIGNA L CURRENT SIGNAL 1 V Out I Out + 2 A1 Ground I Out - 3 V Out I Out + 4 A2 Ground I Out - 5 V Out I Out + 6 A3 Ground I Out - 7 V Out N/A 8 A4 Ground N/A Additionally A1 , A 2[...]

  • Page 29

    Teledyne API Model M201E NH 3 Analyzer Operator Manual Config urable Analog Output Overview 05206H DCN5910 27 3.1 A NALOG O UTPUT - E LECTRONIC C ONFI GURATION The final step in configuring the analy zer’s fo ur analog output channels is to set the electronic signal type and r ange of each channel. This consists of:  Selecting an output type f[...]

  • Page 30

    Configurable Analog Outpu t Overview Teledyne API Model M201E NH 3 Analyzer Operator Manual 28 05206H DCN5910 3.2 A NALOG O UTPUT S IGNAL T YP E AND R ANGE S ELECTION To select an analog output signal type (DC voltag e or current) for one of the analyzer analog output channels press SETUP - MORE -DIA G - 818…ENTER- NEXT…NEXT: DI A G A NA LO G I[...]

  • Page 31

    Teledyne API Model M201E NH 3 Analyzer Operator Manual Config urable Analog Output Overview 05206H DCN5910 29 3.3 S ELECTING A UTO O R M ANUAL A NALOG O UTPUT C ALIBRATIO N The analog outputs configured for vo ltage mode can be calibrated either automatically or manually. In its default mode the instru ment is configured for automatic calibration. [...]

  • Page 32

    Configurable Analog Outpu t Overview Teledyne API Model M201E NH 3 Analyzer Operator Manual 30 05206H DCN5910 D IAG A IO DATA _OUT_ 2 AUTO CAL: O N ON ENT R EX IT E xi t to Re tu r n to th e m a i n S am ple Di s p la y DI AG ANALO G I / O C O NFI G U RA T I O N PR E V NE XT ENT R EX IT DI AG A I O AO UTS CALIBRATED: NO < S ET SE T> CAL EX IT[...]

  • Page 33

    Teledyne API Model M201E NH 3 Analyzer Operator Manual Config urable Analog Output Overview 05206H DCN5910 31 To calibrate the output channels as a group press the following, ( Note: this is the recommended calibration approach): D IAG AIO AU T O CALI BRA TI NG DAT A _ O UT _ 1 AU TO CA LI B RATI NG DAT A_ O U T_2 … AU TO CA LI B RATI NG DAT A _ [...]

  • Page 34

    Configurable Analog Outpu t Overview Teledyne API Model M201E NH 3 Analyzer Operator Manual 32 05206H DCN5910 3.4 M ANUALLY C ALIBRATING A NALOG O UTPUT S IGNA L L EVELS The analog outputs in volt age mode can be manually calibrated to closely match the characteristics of the da ta recorder. Outputs conf igured for 0.1V full scale should always be [...]

  • Page 35

    Teledyne API Model M201E NH 3 Analyzer Operator Manual Config urable Analog Output Overview 05206H DCN5910 33 To make these adjust ments the aut o ca libration feature “DATA_O UT_1 AUTO CAL: OFF” must be turned off for each output channel then press the following: DI A G AIO DATA_O UT _1 C A LIB RA TE D : Y ES < SE T CA L E XI T DI A G A NAL[...]

  • Page 36

    Configurable Analog Outpu t Overview Teledyne API Model M201E NH 3 Analyzer Operator Manual 34 05206H DCN5910 3.5 A NALOG O UTPUT R ECORDER O FFSET A DJUSTMENT An offset can be added to in dividual output channels by pressing the following: D I AG AI O RE CO RD OFF S E T : 0 M V + 0 0 0 0 E N T R EXI T DI A G A NALO G I / O CO NFI G U RATI O N PR E[...]

  • Page 37

    05206H DCN5910 35 4.0 MAINTENANCE SCHEDULE The maintenance requirement s of the M201E are the same as a st andard M200E NO x analyzer but with additiona l maintenance items ( Table 4-1 ). Please refer to Section 13 in the M200E O perator Manual for the M200E maintenance schedule and for maintenance and repair procedures. The M201E requires the foll[...]

  • Page 38

    Maintenance Schedule Teledyne API Model M201E NH 3 Analyzer Operator Manual 36 05206H DCN5910 Table 4-2. M501 NH 3 Converter Rebuild Parts List Part No. Description KIT000193 RETROFIT, M501NH INNER TUBE w/SCREEN KIT000139 REBUILD, CERAMIC BUSHINGS, M501NH HE0000007 CERAMIC HEATER, 220W@60V M501XX 4.2 R EPLACING THE C ATALYTIC C ARTRIDGE 1. Turn off[...]

  • Page 39

    Teledyne API Model M201E NH 3 Analyzer Operator Manual Maintena nce Schedule 05206H DCN5910 37 4.3 R EPLACING THE T HERMOCOUPL E The following instructions provide the necessary information to replace the existing thermocouple. Figure 4-2 is provided for reference. You must obtain the following repl acement parts kit from T-API:  010820000 , Typ[...]

  • Page 40

    Maintenance Schedule Teledyne API Model M201E NH 3 Analyzer Operator Manual 38 05206H DCN5910 2. Remove the cover from the Converter chassis. 3. Unscrew the (4) nuts that secure the front panel to the chassis. They are located just behind the Front Panel along the top. 4. Lower the Front Panel to gain easier access to t he end of the quartz tube. 5[...]

  • Page 41

    Teledyne API Model M201E NH 3 Analyzer Operator Manual Maintena nce Schedule 05206H DCN5910 39 4.4 A UTO Z ERO F LOW C HECK Since the M201E is an ammonia analyzer, t he flow through t he AutoZero orifice is especially important. Check t he AutoZ ero flow as follows: 1. This procedur e should be perfor med wit h the sample pump running. 2. Remove th[...]

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    Maintenance Schedule Teledyne API Model M201E NH 3 Analyzer Operator Manual 40 05206H DCN5910 This page intentionally left blank.[...]

  • Page 43

    05206H DCN5910 41 5.0 ALARMS AND CAUTIONS A functional block diagram of the analyzer is shown in Figure 5-1. 5.1 A LARM During init ial warm up the internal Zer o /Span factory option may exhibit a “Block Temperatur e” warning. This can be clea red once the blo ck temperature stab ilizes at 50 degrees Celsius. The block temper ature is the actu[...]

  • Page 44

    Alarms and Cautions Teledyne API Model M201E NH 3 Analyzer Operator Manual 42 05206H DCN5910 M501NH NH3 CONVERTER CONVERTER MOLYBDENUM DFU FILTER NAFION DRIER GENERATOR OZONE SAMPLE MANIFOLD PHOTONS REACTION CELL MOTHERBOARD I/O I/O OUTPU TS ANALOG DIGI TAL ANALOG PREAMP BUS STD AUTOZERO TNx / NOx VALVE VALV E DESTRUCT OZONE VACUUM PUMP RS-232 SCRU[...]

  • Page 45

    05206H DCN5910 43 6.0 M201E SPARE PARTS LIST While this section lists the sp are parts for the M201E, it is recommended that you refer to our Website or Sales for updates. M201E Spare Parts List, Source: PN 06185H (DCN5494) Part Number Description 000940100 CD, ORIFICE, .003 GREEN 000940400 CD, ORIFICE, .004 BLUE 000940500 CD, ORIFICE, .007 ORANGE [...]

  • Page 46

    M201E Spare Parts List Teledyne API Model M201E NH 3 Analyzer Operator Manual 44 05206H DCN5910 M201E Spare Parts List, Source: PN 06185H (DCN5494) Part Number Description 046030000 AKIT, CH-43, 3 REFILLS 048620200 PCA, SERIAL INTERFACE, w/ MD, E SERIES (USE WITH ACROSSE R CPU 041710000) 049310100 PCA, TEC DRIVER, PMT, M100/200, E SERIES 051211000 [...]

  • Page 47

    Teledyne API Model M201E NH 3 Analyzer Operator Manual M201E Spa re Parts List 05206H DCN5910 45 M201E Spare Parts List, Source: PN 06185H (DCN5494) Part Number Description OR0000039 ORING, 2-012V OR0000044 ORING, 2-125V OR0000083 ORING, 105M, 1MM W X 5 MM ID, VITON OR0000086 ORING, 2-006, CV-75 COMPOUND(KB) OR0000094 ORING, 2-228V, 50 DURO VITON(K[...]

  • Page 48

    M201E Spare Parts List Teledyne API Model M201E NH 3 Analyzer Operator Manual 46 05206H DCN5910 This page intentionally left blank.[...]

  • Page 49

    05206H DCN5910 47 7.0 CALCULATING MOLY CONVERTER EFFICIENCIES 7.1 P URPOSE To provide instructions on how t o calcul ate the efficiency of a Moly converter when using a GPT method of testing converters, by using the US EPA method, where the actual concentration of ozone is not a factor in the accuracy of the calculation of the converter efficiency.[...]

  • Page 50

    Calculating Moly Converter Efficiencies Teledyne API Model M201E NH 3 Analyzer Operator Manual 48 05206H DCN5910 5. Remove the converter bypass and install the converter back into the NOx sample stream, such that the NO sample goes through the converter again and allow th e machine to stabilize. Write down your NOx value on your data sheet on line [...]

  • Page 51

    05206H DCN5910 49 MOLY TEST DATA SHEET L i n e # T E S T RESULT 2 LEAK-CHECK (WHEN HOT) YES / NO 3 NO X RESPONSE (MOLY BYPASSED) ___ _______ 4 NO X RESPONSE (MOLY IN-LINE ) ___ _______ 5 OUT-GAS SING / EAT ING (NO – NO X ) __________ (>-5 PPB, <5 PPB) 6 (NOx ORIG ) (NO X mode, O 3 off) __________ PPB 7 (NOx REM ) (NO X mode, O 3 on) _______[...]